KMID : 1007520120210030853
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Food Science and Biotechnology 2012 Volume.21 No. 3 p.853 ~ p.858
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Inter-laboratory Study to Define the Temperature Interval for a Thermoluminescence Heating Unit Used to Identify Irradiated Food
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Ahn Jae-Jun
Kashif Akram Baek Ji-Yeong Kim Yeon-Joo Kim Moon-Young Jeong Il-Yun Kwon Joong-Ho
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Abstract
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EN 1788:2001 suggests defining the temperature range for the thermoluminescence (TL) heating unit to calculate the TL ratio (TL1/TL2). In the present study, practical temperature ranges were established by using well-characterized lithium fluoride (LiF, TLD-100¢ç) at 4 different research institutes in Korea. Temperature ranges differed according to models of TLD heating unit, which were wide in the case of RIS¨ª (160-249¡ÆC) as compared with Harshaw (155-232oC) TLD readers. The silicate minerals separated from irradiated turmeric samples were measured to check these intervals on a practical basis. The X-ray diffraction (XRD) analysis of separated minerals showed that quartz and feldspar minerals were the main source of well-characterized TL glow curve following irradiation. The TL glow peaks from the separated minerals were narrower in Harshaw than RIS¨ª TLD readers. The TL ratios determined after re-irradiation (1 kGy) for the tested minerals, using the pre-defined temperature intervals, provided the satisfactory results.
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KEYWORD
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irradiation, identification, lithium fluoride, turmeric
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